Chemistry 211, Schedule for Semester I, Fall 2011

Week	Dates	Experiment #	Experiment Title	Experiment Type
General Lab Information (docx) (pdf) Forces and Factors (docx) (pdf) Laboratory Equipment
1	9/02 - 9/05		No lab meeting this week.
2	9/09 - 9/12	Fractional Distillation and Gas Chromatography (docx) (pdf)	General Lab Information Gas Chromatography/Steam Distillation Check-in YouTube General safety: Chemical exposure: Fire safety: Thermal Cuts and Burns: How to Build a Proper Still: part I How to Build a Proper Still: part II How to Run a Basic GC Images Apparatus 1 Apparatus 2	I ^{1, 2}
3	9/16 - 9/19	Fractional Distillation/Simple Distillation (docx) (pdf)	Fractional Distillation/Simple Distillation YouTube Recrystallization	I ^{1, 2}
5	9/23 - 9/26	Recrystallization and Melting Point Determination: Yield vs. Purity (docx) (pdf)		I ²
6	9/30 - 10/03	Extraction of Caffeine from Tea (docx) (pdf)	Recrystallization and Melting point YouTube YouTube on separation of acids and bases How to Flute Filter Paper How to pack a melting point capillary and measure a melting point Rotary Evaporation: part I Rotary Evaporation: part II Sublimation Some Instruction on how to do the arrow formalism soxhlet extraction	I, G
8	10/07 - 10/10	Introduction to Spectroscopy(doc) (pdf) D₂O Addition of Fumarate to Produce Malate Set-up Rxn(pdf)	Introduction to Spectroscopy D₂O Addition of Fumarate to Produce Malate Set-up Rxn YouTube Making up samples for IR and running new FTIRS Melting point depression and broadening IR-1 basics important for fall IR-2 IR-3 IR-4 IR-5 important for fall How to prepare sample for NMR How to Inject a Sample into the NMR at Bryn Mawr College How to Run NMR Sample at Bryn Mawr College part I How to Run NMR Sample at Bryn Mawr College part II How to solve a basic NMR Problem A practice NMR problem A practice NMR problem Solution to basic nmr problem no. 3 Solution to NMR Problem no. 4 Spectroscpy as Imagery Running NMR part 3 Melting point depression and broadening Run NMR	I, G
7	10/14 - 10/17		Fall Break, rest, eat, have fun
9	10/21 - 10/24	Experiment 4 (DOC) (PDF) Introduction to Spectroscopy (Continued)(pdf) D₂O Addition of Fumarate to Malate Run NMR (docx)	Introduction to Spectroscopy (Continued) D₂O Addition of Fumarate to Malate Run NMR	I,G
	10/28 - 10/31	Friedel Crafts Kinetic PDF DOC Friedel Crafts Part II Thermo PDF DOC	Friedel Craffs: Part I Kinetic Control vs. Friedel Crafts Part II Thermo PDF Workshop Intro to Mass Spec Quiz 1 Spectroscopy	C
10	11/4 - 11/7	Determinaton of the Stereochemistry of the Fumarase Induced Conversion of Fumarate to Malate (pdf)	Conference on D₂O Addition of Fumarate and on Thermodynamic Friedel Crafts/GCMS More Workshop Intro to Mass Spec	C
11	11/11 -11/14	Green Synthesis of a Flourescent Natural Product	Green Synthesis of a Flourescent Natural Product Synthesis of 4-umbelliferone More Workshop Intro to Mass Spec	P,F
	11/18 - 11/21	S_N2 for Pechman	S_N2 for Pechman S_N2 Reacton of 4-umbelliferone TLC and Column Chromatography Nerz Notes for Week_of November_17 Worksheet for Total Synthesis of 7
12	11/26 - 11/30		Thanksgiving Week, Make-up Days
13	12/02 - 12/05	Oxidation of Isoborneol to Camphor (PDF)	Oxidation of Isoborneol to Camphor On Thermodynamic Friedel Crafts	2
15			YouTube How to Make a Micro-drying Apparatus Conference during Lab
	11/09 - 12/12		Make up week Quiz 2

PR	Prelab only
C	Conference on results and postlab with instructor
P	Preparative experiment/write-up
I	Investigative experiment/write-up
F	Form write-up
G	Group experiment/write-up. Only one report per group.
1	There will be one report written for two parts of this experiment.
2	Limited write up. See specific instructions in lab book.