BRYN MAWR COLLEGE
Organic Chemistry Laboratory
Chemistry 211
Schedule for Semester I, Fall 2013
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Home Page Office Hours Chem 211 Schedule Chem 211 General Useful Web Sites
Week Dates Experiment # Experiment Title Experiment Type
General Lab Information (docx) (pdf)
Forces and Factors (docx) (pdf)
Laboratory Equipment
1 9/02 - 9/05   No lab meeting this week.  
2 9/09 - 9/12

Fractional Distillation and Gas Chromatography (docx)
(pdf)

General Lab Information
Gas Chromatography/Steam Distillation
Check-in
3 9/16 - 9/19 Fractional Distillation/Simple Distillation (docx) (pdf)
Fractional Distillation/Simple Distillation
5 9/23 - 9/26 Recrystallization and Melting Point Determination: Yield vs. Purity (docx) (pdf)
6 9/30 - 10/03 Extraction of Caffeine from Tea (docx)
(pdf)


Recrystallization and Melting point
8 10/07 - 10/10 Introduction to Spectroscopy(doc) (pdf)

D2O Addition of Fumarate to Produce Malate Set-up Rxn(pdf)
Introduction to Spectroscopy
D2O Addition of Fumarate to Produce Malate Set-up Rxn
7 10/14 - 10/17 Fall Break, rest, eat, have fun
9 10/21 - 10/24 Experiment 4 (DOC) (PDF)
Introduction to Spectroscopy (Continued)(pdf)
D2O Addition of Fumarate to Malate Run NMR (docx)
Introduction to Spectroscopy (Continued)
D2O Addition of Fumarate to Malate Run NMR
  10/28 - 10/31
Friedel Crafts Part II Thermo
PDF

Workshop Intro to Mass Spec
Quiz 1 Spectroscopy
C
10 11/4 - 11/7 Determinaton of the Stereochemistry of the Fumarase Induced Conversion of Fumarate to Malate (pdf)
Conference on D2O Addition of Fumarate and on Thermodynamic Friedel Crafts/GCMS
More Workshop Intro to Mass Spec
11 11/11 -11/14 Green Synthesis of a Flourescent Natural Product Green Synthesis of a Flourescent Natural Product
Synthesis of 4-umbelliferone
More Workshop Intro to Mass Spec
P,F
  11/18 - 11/21 SN2 for Pechman SN2 for Pechman
SN2 Reacton of 4-umbelliferone

TLC and Column Chromatography
Nerz Notes for Week_of November_17
Worksheet for Total Synthesis of 7
 
12 11/26 - 11/30   Thanksgiving Week, Make-up Days  
13 12/02 - 12/05

Oxidation of Isoborneol to Camphor
(PDF)

Oxidation of Isoborneol to Camphor
On Thermodynamic Friedel Crafts
2
15    
YouTube
Conference during Lab
  11/09 - 12/12   Make up week
Quiz 2
 

PR Prelab only
C Conference on results and postlab with instructor
P Preparative experiment/write-up
I Investigative experiment/write-up
F Form write-up
G Group experiment/write-up.  Only one report per group.
1 There will be one report written for two parts of this experiment.
2 Limited write up. See specific instructions in lab book.
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